HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Amino-4-phenylethynyl-phenyl)-carbamic acid tert-butyl ester → HCID 86588015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Amino-4-phenylethynyl-phenyl)-carbamic acid tert-butyl ester | HCID 11404065 | — |
| Reactant | 6-(3-Imidazol-1-yl-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one | HCID 22224895 | — |
| Product | HCID 86588015 | HCID 86588015 | 68.8% |
Reaction Steps
Prepared from (2-amino-4-phenylethynyl-phenyl)-carbamic acid tert.-butyl ester (Example G2) (154 mg, 0.5 mmol) and 6-(3-imidazol-1-yl-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one (Example J10) (135 mg, 0.5 mmol) according to the general procedure K. Obtained as an orange oil (179 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07151098B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-936cb189b8294fe4b84070ad074d221b |
| Source note | uspto-grants-2006_12 |