HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 10343002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 11682666 | HCID 11682666 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10343002 | HCID 10343002 | — |
Reaction Steps
Reaction of cyclohexanesulfonic acid {4-[4-(3-amino-phenyl)-piperazin-1-yl]-butyl}-amide and acetyl chloride in dichloromethane as described in Example 3 gave the desired product, N-{3-[4-(4-Cyclohexanesulfonylamino-butyl)-piperazin-1-yl]-phenyl}-acetamide, as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153858B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-916884686e6c4ae0ae482239a46f8ce4 |
| Source note | uspto-grants-2006_12 |