HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 17954522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178488024 | HCID 178488024 | — |
| Product | HCID 17954522 | HCID 17954522 | 61% |
Reaction Steps
Prepared using general procedure 3; 6-Methoxy-2-hydroxy-4-(3,4-dichlorophenyl)aminoquinoline (1.05 g, 3.13 mmol) and 26 mL of POCl3 were heated to 120° C. for 4 h. Isolation afforded 0.685 g of material (1.94 mmol, 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153865B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-248ecc8b5c6f428aab0379b88cb0256c |
| Source note | uspto-grants-2006_12 |