HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69666214, compound → HCID 69666423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69666214 | HCID 69666214 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69666423 | HCID 69666423 | — |
Reaction Steps
The alkene 7-7 (1.02 g, 1.74 mmol) was dissolved in EtOH (50 mL) and degassed with argon. Palladium on carbon (10%; 100 mg) was added and the mixture stirred under an atmosphere of hydrogen gas (balloon) for 3 hours. The mixture was filtered through celite and the solvent removed to give the title compound 7-8 which was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153862B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-37432d75052b49548fff0b5992029725 |
| Source note | uspto-grants-2006_12 |