HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodo-2-methylpyridine → HCID 69120171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodo-2-methylpyridine | HCID 12691322 | — |
| Reactant | HCID 85997994 | HCID 85997994 | — |
| Product | HCID 69120171 | HCID 69120171 | — |
Reaction Steps
4-[1-(3,4-Dichloro-phenyl)-2-methyl-1H-imidazol-4-ylethynyl]-2-methyl-pyridine hydrochloride (2) [MS: m/e=341.9 (M+H+)] was prepared in analogy to the method as described in Example 1 Method B starting from 1-(3,4-dichloro-phenyl)-4-ethynyl-2-methyl-1H-imidazole (IV-2) and 4-iodo-2-methyl-pyridine. For further purification the compound was precipitated as its HCl salt from an etheral solution. Method C:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153874B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-d216625d266d481e80d1264618039543 |
| Source note | uspto-grants-2006_12 |