HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 86591157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 69019837 | HCID 69019837 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86591157 | HCID 86591157 | — |
Reaction Steps
A mixture of intermediate (4) (0.0161 mol) and NaN3 (0.0161 mol) in methanol (25 ml) was stirred and refluxed overnight.The product was used without further purification, yielding 2-azido-N-[2-(3-chlorobenzoyl)-4-[(4-chlorophenyl)hydroxy(1-methyl-1H-imidazol-5-yl)methyl]phenyl]-acetamide (intermediate 5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153958B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-0accd08af5104bdca9787c8d0a78dea3 |
| Source note | uspto-grants-2006_12 |