HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 69021506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | HCID 69023059 | HCID 69023059 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 69021506 | HCID 69021506 | 203.2% |
Reaction Steps
A mixture of intermediate (17) (0.0269 mol) and mercapto-acetic acid (0.0269 mol) in HCl 6N (150 ml) was stirred and refluxed for 2 hours and brought to room temperature. The solvent was evaporated till dryness, yielding 15 g (96%) of [[[2-amino-5-[(4-chlorophenyl)(1-methyl-1H-imidazol-5-yl)methyl]phenyl](3-chlorophenyl)methyl]thio]-acetic acid hydrochloride salt (intermediate 18).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153958B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-0b1f67d56d3d4bcd8c957bf5373c8fdc |
| Source note | uspto-grants-2006_12 |