HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 45087000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 5-Bromo-N-cyclopropylpyridine-3-carboxamide | HCID 604228 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 45087000 | HCID 45087000 | — |
Reaction Steps
Prepared according to the procedure described in EXAMPLE 9 (Step 4) but using 5-bromo-N-cyclopropyl-nicotinamide from Step 1 as starting material. Flash chromatography (EtOAc:MeOH; 9:1) afforded the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153968B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-b996ee0a3c5a46e6a64046a2e9bbd224 |
| Source note | uspto-grants-2006_12 |