HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69373820, compound → HCID 69375686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69373820 | HCID 69373820 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69375686 | HCID 69375686 | — |
Reaction Steps
To a solution of (5-bromo-pyridin-2-yl)-(4-methoxy-phenyl)-methanol (1.0 eq.) in EtOAc (0.2M) was added MnO2 (3.0 eq.). The mixture was stirred for 1 h, filtered on celite and concentrated to afford the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07153968B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-e140339956ab4924a9d9fa05b001ff55 |
| Source note | uspto-grants-2006_12 |