HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19704248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86752027 | HCID 86752027 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19704248 | HCID 19704248 | 92.7% |
Reaction Steps
305 mg of the product of Stage B and 1.75 ml of trifluoroacetic acid were heated at 40° C. for 12 hours in 6.1 ml of dichloromethane. The mixture was poured into water, sodium bicarbonate was added until a pH of 6-7 was obtained. Extraction was carried out with methylene chloride and the solvent was eliminated under reduced pressure to obtain 180 mg of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05714508 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-59298bb53f4d4d5eb769ea9d646c77bd |
| Source note | uspto-grants-1998_02 |