1-Iodopropane → HCID 22619457, compound
Reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([Br:12])[CH:8]=[CH:9][C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].I[CH2:14][CH2:15][CH3:16]>>[C:1]([C:5]1[CH:6]=[C:7]([Br:12])[CH:8]=[CH:9][C:10]=1[O:11][CH2:14][CH2:15][CH3:16])([CH3:4])([CH3:2])[CH3:3]Participants
3
Procedure
Following the basic procedure of Example 46(a), by reacting 4.58 g (0.02 mol) of 3-tert-butyl-4-hydroxybromobenzene with 2.2 ml (0.022 mol) of 1-iodopropane, 4.7 g (87%) of 3-tert-butyl-4-propyloxybromobenzene were obtained in the form of a colorless oil.
Sources & evidence
- ORD record
- ord-82f45e1aedba4a97a8a2af46abc312cd
- Source dataset
- uspto-grants-1998_02
- Patent number
- US05716624
Reaction notes
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