HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 54010371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 1-(Bromomethyl)-4-nitronaphthalene | HCID 12749163 | — |
| Product | HCID 54010371 | HCID 54010371 | — |
Reaction Steps
1-Bromomethyl-4-nitronaphthalene and triethylphosphite ((C2H5 O)3P) were treated in the same manner as in Reference Example 43 to yield diethyl (4-amino-1-naphthyl)methylphosphonate, which was then recrystallized from ethyl acetate-hexane to yield yellow prisms having a melting point of 73°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716944 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-c421f90753d44f4bae1116845c78c40c |
| Source note | uspto-grants-1998_02 |