HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 19700656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Cornforth reagent | HCID 2724130 | — |
| Reactant | HCID 19700735 | HCID 19700735 | — |
| Product | HCID 19700656 | HCID 19700656 | — |
Reaction Steps
2-(Hydroxymethyl-3-chlorophenyl)-3-carboxypyridine was dissolved in a solution of methylene chloride/glacial acetic acid (5:1). Pyridinium dichromate (10.95 g, 29 mmoles) was added and the solution was stirred at room temperature under an inert atmosphere. The solvent was removed yielding 2-(3-chlorobenzoyl)-3-carboxypyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716954 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-e8177298a6d94f14a8fcb0471ccd25c7 |
| Source note | uspto-grants-1998_02 |