Thionyl Chloride → HCID 15233867, compound

HRID 861982Notes

Reaction equation

HRID 861982 reaction equation
O[CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[N:7]([CH:9]=[C:10]([C:12]([O:14][CH2:15][CH3:16])=[O:13])[N:11]=2)[CH:8]=1.O=S(Cl)[Cl:19]>C(Cl)(Cl)Cl>[Cl:19][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[N:7]([CH:9]=[C:10]([C:12]([O:14][CH2:15][CH3:16])=[O:13])[N:11]=2)[CH:8]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 19701264HCID 19701264, compound

Product 1

HCID 15233867HCID 15233867, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

By the method of Example 5, the product from Example 10 (2.52 g, 11.4 mmol) dissolved in CHCl3 (100 mL) was reacted with SOCl2 (1.5 g, 12.6 mmol). Final workup provided 2.66 g (98%) of title compound.

Sources & evidence

ORD record
ord-8234422aebea4866bbf9b894e7eb7875
Source dataset
uspto-grants-1998_02
Patent number
US05716964

Reaction notes

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