HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15233867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19701264 | HCID 19701264 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 15233867 | HCID 15233867 | 98% |
Reaction Steps
By the method of Example 5, the product from Example 10 (2.52 g, 11.4 mmol) dissolved in CHCl3 (100 mL) was reacted with SOCl2 (1.5 g, 12.6 mmol). Final workup provided 2.66 g (98%) of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716964 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-8234422aebea4866bbf9b894e7eb7875 |
| Source note | uspto-grants-1998_02 |