Hydrazine hydrate (1:1) → HCID 86752042, compound

Participants

Reaction Steps

The product from Example 15 (1.4 g, 3.7 mmol) was dissolved in CH2 Cl2 (10 mL) and placed in a 25 mL flask. Hydrazine monohydrate (0.187 g, 3.7 mmol) was added to the flask, and the reaction was allowed to stir at room temperature for 2 h. Two additional equivalents of hydrazine monohydrate were added to drive the reaction to completion. Filtering and solvent removal under reduced pressure gave 0.87 g of crude title compound which was used without further purification.

Provenance & Evidence