HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 131720463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | Ethyl 5-(diethoxyphosphinyl)imidazo[1,2-a]pyridine-2-carboxylate | HCID 19701110 | — |
| Reactant | HCID 19701381 | HCID 19701381 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131720463 | HCID 131720463 | — |
Reaction Steps
The product from Example 51 (1.6 g, 4.4 mmol) was dissolved in CH2 Cl2 (30 mL), treated with activated charcoal and filtered. To this filtrate was then added 6N HCl in dioxane (0.9 mL, 4.4 mmol) followed by Et2O (100 mL). The precipitated product was filtered, washed with Et2O, and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05716964 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-756be3881f944587ac22bb3e422c4239 |
| Source note | uspto-grants-1998_02 |