HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 11332776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 11332776 | HCID 11332776 | 69% |
Reaction Steps
A quantity of 121 g of N-benzylmethylamine was reacted with 100 g of acryloyl chloride in the presence of 111 g of triethylamine in ether at 0° C. to 25° C. for 16 hours. The product was filtered, the solvent was removed, and N-benzyl-N-methylacrylamide was isolated in 69% yield by distillation under vacuum Cop 83°-85° C./0.04 mm--Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05717049 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-5d884696b0bb473c86c0aa0f8a85f9ce |
| Source note | uspto-grants-1998_02 |