HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N,N,N-Triethyl-2-hydroxyethan-1-aminium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethanol, 1-bromo- | HCID 14202443 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N,N,N-Triethyl-2-hydroxyethan-1-aminium bromide | HCID 15419000 | 41% |
Reaction Steps
Hydroxyethyltriethylammonium bromide was obtained as follows: ##STR14## Bromoethanol (distilled, 2 g, 16 mmole) and triethylamine (1.62 g, 16 mmole) were heated in dichloromethane (30 ml) at 40° C. for 16 hours. After cooling the precipitate was filtered and dried over phosphorus pentoxide to yield hydroxyethyltriethylammonium bromide as a white powder, 1.47 g, 6.5 mmole, 41% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05717047 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-ce3fd3ecd882480d8c88a83381d44cb1 |
| Source note | uspto-grants-1998_02 |