HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid → N-[1-(3,5-Dimethoxyphenyl)-1-methylethyl]-3-cyanoandrosta-3,5-diene-17beta-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid | HCID 15380254 | — |
| Edukt | 2-(3,5-Dimethoxyphenyl)propan-2-amine | HCID 15754138 | — |
| Produkt | N-[1-(3,5-Dimethoxyphenyl)-1-methylethyl]-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 57001892 | 98% |
Reaktionsschritte
Following a procedure similar to that described in Preparation 16a, but using 3-cyanoandrosta-3,5-diene-17β-carboxylic acid [prepared as described in Example 1(b)] and 1-(3,5-dimethoxyphenyl)-1-methylethylamine as starting materials, in relative proportions similar to those used in that Preparation, the title compound was obtained in a yield of 98%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05717088 |
| Quelldatensatz | uspto-grants-1998_02 |
| ORD ID | ord-a744a9b9026d438fa76e580f7dc1606b |
| Quellennotiz | uspto-grants-1998_02 |