HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 70051448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | HCID 15379623 | HCID 15379623 | — |
| Product | HCID 70051448 | HCID 70051448 | 94% |
Reaction Steps
By condensing 3-amino-1,3-dihydro-1-methyl-5-(2,4,6-trimethoxyphenyl)-1,4-benzodiazepin-2-one with 3-methylphenyl isocyanate, 1,3-dihydro-1-methyl-3-(3-methylphenylureido)-5-(2,4,6-trimethoxyphenyl)-1,4-benzodiazepin-2-one is obtained; m.p.=240° C., Yield=94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719143 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-98fdd29b41d64a7cb0a9cbc7098ef389 |
| Source note | uspto-grants-1998_02 |