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HRID862452

反应详情

EQUATION

反应方程式

HRID 862452 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C1CCCNC1
HCID4498

3-​Piperidinecarboxylic acid

C6H11NO2

结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

PRODUCTS

生成物

1
结构：CC(=O)N1CCCC(C(=O)O)C1
HCID14043896

1-Acetyl-3-piperidinecarboxylic acid

C8H13NO3

收率 97.4%

PROCEDURE

实验过程

Nipecotic acid (3.87 grams) (30.0 mmoles) was reacted with acetic anhydride (9.17 grams) (90 mmoles) as described in Preparative Example 13A to give the title compound (Yield: 5.0 grams, 97%, MH+ 172).