HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nipecotic Acid → 1-Acetyl-3-piperidinecarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nipecotic Acid | HCID 4498 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Product | 1-Acetyl-3-piperidinecarboxylic acid | HCID 14043896 | 97.4% |
Reaction Steps
Nipecotic acid (3.87 grams) (30.0 mmoles) was reacted with acetic anhydride (9.17 grams) (90 mmoles) as described in Preparative Example 13A to give the title compound (Yield: 5.0 grams, 97%, MH+ 172).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719148 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-6ff3c41c4f3340fca0f1971a9bc18256 |
| Source note | uspto-grants-1998_02 |