HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 23287291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2,3-Dimethylimidazo[1,2-a]pyridin-8-ol | HCID 22467949 | — |
| Reactant | HCID 53835417 | HCID 53835417 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 23287291 | HCID 23287291 | 22.5% |
Reaction Steps
Analogously to Example 5, 2.0 g (12.4 mmol) of 8-hydroxy-2,3-dimethylimidazo[1,2-a]pyridine, 3.6 g (13.9 mmol) of 2-methoxyethyl 2-chloromethyl-3-methylphenylcarbamate, 0.18 g of sodium iodide and 1.3 g of sodium carbonate are reacted in 30 ml of acetone. 1.07 g (22.5%) of the title compound of m.p. 107°-108° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719161 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-f7f1d8d83cd54a109265d4d6196f651a |
| Source note | uspto-grants-1998_02 |