HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(3-tert-butoxycarbonylaminomethyl-6-nitrophenyl)propionate → HCID 19698388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(3-tert-butoxycarbonylaminomethyl-6-nitrophenyl)propionate | HCID 19698374 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19698388 | HCID 19698388 | 116.1% |
Reaction Steps
A solution of methyl 3-(3-tert-butoxycarbonylaminomethyl-6-nitrophenyl)propionate (3.2 g, 9.5 mmol) in ethyl acetate (35 mL) in the presence of 10% Pd/C was hydrogenated under atmospheric pressure of hydrogen at room temperature. The catalyst was removed by filtration by using celite and the filtrate was concentrated to give 3.4 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719152 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-885d8d7adc9e429290e31bd9c34ed316 |
| Source note | uspto-grants-1998_02 |