HRID862582

反应详情

EQUATION

反应方程式

HRID 862582 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of methyl 3-(3-tert-butoxycarbonylaminomethyl-6-nitrophenyl)propionate (3.2 g, 9.5 mmol) in ethyl acetate (35 mL) in the presence of 10% Pd/C was hydrogenated under atmospheric pressure of hydrogen at room temperature. The catalyst was removed by filtration by using celite and the filtrate was concentrated to give 3.4 g of the title compound.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. concentrationthe filtrate was concentrated