HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 2797868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | α-Phenyl-4-pyridinemethanol | HCID 98305 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 2797868 | HCID 2797868 | — |
Reaction Steps
To a solution of 27.75 g (0.15 mol) of (4-pyridyl)benzyl alcohol and 200 ml of chloroform is run in dropwise, at room temperature, a solution of 15.25 ml (0.2 mol) of SOCl2 and 50 ml of CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719168 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-d10fc50f700d493ab1ed685d939c5f84 |
| Source note | uspto-grants-1998_02 |