反应详情

To a suspension of 15.44 g (0.06 mol) of benzhydrylsulphinylacetic acid in 90 ml of methylene chloride are added 6.48 g (0.06 mol, i.e. 6.17 ml) of 2-aminomethylpyridine and 12.36 g (0.06 mol) of dicyclohexylcarbodiimide are added to the solution thus obtained. The mixture is heated at reflux for about 3 to 4 hours, then left to cool.

1. additionare added to the solution
2. customthus obtained
3. temperatureThe mixture is heated
4. temperatureat reflux for about 3 to 4 hours
5. waitleft
6. temperatureto cool