Hydrochloric Acid → HCID 21849322, compound
Reaction equation
[ClH:1].Cl.[NH2:3][C:4]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([O:22]C)=[O:21])([CH2:7][OH:8])[CH2:5][OH:6]>>[ClH:1].[NH2:3][C:4]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])([CH2:7][OH:8])[CH2:5][OH:6]Participants
3
Conditions
- Temperature
- 90 °C
Procedure
2N Hydrochloric acid (0.5 ml) was added to 10 mg of 2-amino-2-(11-methoxycarbonylundecyl)-1,3-propanediol hydrochloride and the mixture was heated at 90° C. for 1 hour. The solvent was distilled away under reduced pressure to give 10 mg of the subject compound.
Workup
- distillationThe solvent was distilled away under reduced pressure
Sources & evidence
- ORD record
- ord-e8bdefea088444508e131d649a5d30c8
- Source dataset
- uspto-grants-1998_02
- Patent number
- US05719176
Reaction notes
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