HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenyl formate → HCID 19697842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenyl formate | HCID 74628 | — |
| Reactant | 2-(Aminomethyl)aniline | HCID 178096 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19697842 | HCID 19697842 | — |
Reaction Steps
The amine component employed is prepared by reaction of 2.6 g of 2.6 g of 2-(aminomethyl)aniline, dissolved in 50 ml of methylene chloride, with 3.91 g of 4-nitrophenyl formate at room temperature for 4 h. Purification over 250 g of silica gel (mobile phase N) gives 2-(formylaminomethyl)aniline: Rf (N)=0.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719141 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-06f3f0f8b54142149fdeeb9c52a2dca3 |
| Source note | uspto-grants-1998_02 |