HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoacetamide → HCID 8176846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoacetamide | HCID 3727 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Phenol, 4-methoxy-2-nitro- | HCID 15285 | — |
| Product | HCID 8176846 | HCID 8176846 | — |
Reaction Steps
Reaction of 1.41 g of 4-methoxy-2-nitrophenol, 3.04 g potassium carbonate and 3.61 g of iodoacetamide analogously to the process described in Example 55) gives 2-carbamoylmethoxy-5-methoxynitrobenzene: mp 190°-1° C.; Rf (O)=0.58; FAB-MS: (M+H)+ =227; anal. calc. for C9H10N2O5 : C47.79%, H4.46%, N12.38%; found C47.90%, H4.48%, N12.58%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05719141 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-6b44def19dbc4b01b0907b0e022e3b85 |
| Source note | uspto-grants-1998_02 |