Methyl chloroformate → HCID 19697544, compound

Participants

Reaction Conditions

Reaction Steps

The title compound is prepared from 3.1 g of 3(R,S)-aminomethyl-1,2,3,4-tetrahydroquinoline and 2.2 ml methyl chloroformate in an analogous manner to that described in Example 54) (stirring for 2 h at 0° C.) and is purified by chromatography over silica gel with a 1:2 mixture of hexane and ethyl acetate as the mobile phase: Rf (A)=0.25; FAB-MS: (M+H)+ =221.

Provenance & Evidence