Acryloyl chloride → HCID 86752135, compound

HRID 863358Notes

Reaction equation

HRID 863358 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][Si:5]([O:12][CH2:13][CH3:14])([O:9][CH2:10][CH3:11])[O:6][CH2:7][CH3:8].C([Cl:19])(=O)C=C>CCOCC>[ClH:19].[NH2:1][CH2:2][CH2:3][CH2:4][Si:5]([O:12][CH2:13][CH3:14])([O:6][CH2:7][CH3:8])[O:9][CH2:10][CH3:11]

Participants

4

Reactant 2

HCID 13140Acryloyl chlorideHCID 13521(3-Aminopropyl)triethoxysilane

Product 1

HCID 86752135HCID 86752135, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

To a solution of 66.3 g of aminopropyl triethoxy silane in 200 ccs of ether, a solution of 13.6 g of acryloyl chloride in 100 ccs of ether was added dropwise at 0° C. The white precipitate of aminopropyl triethoxy silane hydrochloride formed was filtered off by suction whereupon the ether filtrate was concentrated by evaporation and the residue was distilled.

Sources & evidence

ORD record
ord-382b34bcdd1c44a8bdaff551131cd22d
Source dataset
uspto-grants-1998_02
Patent number
US05720840

Reaction notes

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