HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 86752135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86752135 | HCID 86752135 | — |
Reaction Steps
To a solution of 66.3 g of aminopropyl triethoxy silane in 200 ccs of ether, a solution of 13.6 g of acryloyl chloride in 100 ccs of ether was added dropwise at 0° C. The white precipitate of aminopropyl triethoxy silane hydrochloride formed was filtered off by suction whereupon the ether filtrate was concentrated by evaporation and the residue was distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05720840 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-382b34bcdd1c44a8bdaff551131cd22d |
| Source note | uspto-grants-1998_02 |