Ethyl Acetate → HCID 23217743, compound

Participants

Reaction Steps

Compound 13 was prepared from 12 in a similar manner as described for compound 7: TLC (5% EtOAc-95% hexanes) Rf 0.88; 1H-NMR (CDCl3) δ1.30 (m, 6H, CH2CH3 +CH3), 1.34 (s, 18H, 6(CH3)), 2.20, (s, 3H, CH3), 2.40 (m, 2H, CH2), 2.85 (m, 1H, CH), 4.14 (m, 2H, CH2CH3), 5.62 (s, 1H, =CH), 6.03 (m, 2H, =CH), 7.00 (d, J=I Hz, 2H, Ar-H), 7.24 (t, J=1 Hz, 1H, Ar-H).

Provenance & Evidence