HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19430424, compound → HCID 19430414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19430424 | HCID 19430424 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19430414 | HCID 19430414 | 85% |
Reaction Steps
20 g of the compound from Example VI are dissolved in 75 ml of tetrahydrofuran and the solution is added dropwise to 40 mmol of LiAlH4 in 50 ml of tetrahydrofuran. Customary working up gives 85% of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721248 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-38043b263b3b4259b3fc088f4c730a83 |
| Source note | uspto-grants-1998_02 |