HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Hydroxymethyl-2-phenylbenzofuran → 2-Phenyl-benzo[b]furan-7-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Hydroxymethyl-2-phenylbenzofuran | HCID 14514949 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Phenyl-benzo[b]furan-7-carboxaldehyde | HCID 19696480 | — |
Reaction Steps
12 g of manganese dioxide are added to 2 g of 7-hydroxymethyl-2-phenylbenzo [b]furan (prepared according to Example 1 from EP 306 226) in 100 ml of methylene chloride and the mixture is heated under reflux for 1 hour. It is cooled end filtered with suction over a filtering auxiliary, and the filtrate is concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721248 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-6611e79c7f9b4fd9a9df49f5bc7356a7 |
| Source note | uspto-grants-1998_02 |