Hydrochloric Acid → HCID 19696143, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of acetic acid 8-acetylamino-5-bromo-7-nitro-1,2,3,4-tetrahydronaphthalen-2-yl ester (2 g, 5.4 mmol), acetic acid (15 mL) and 6N HCl (30 mL) was stirred at 90° C. for 18 h. The solvent was removed by rotoevaporation to give the product (1.6 g) as an orange solid in quantitative yield.

Provenance & Evidence