Bromine → HCID 19696170, compound

Participants

Reaction Steps

A solution of N-(7-azido-5,6,7,8-tetrahydronaphthalen-1-yl)-acetamide (1 g, 4.3 mmol) in acetic acid (40 mL) was treated dropwise with bromine (1 g, 6.5 mmol) and stirred at room temperature for 3 h. The solvent was evaporated and the solid residue was washed with ether, collected by filtration and dried to give the product (1.5 g) in 89% yield.

Provenance & Evidence