Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 19696172 | HCID 19696172 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19696253 | HCID 19696253 | 80% |
Reaction Steps
N-(5-Acetylamino-6-bromo-4-nitro-indan-2-yl)-acetamide (1 g, 2.8 mmol) was suspended in a 2:1 mixture of sulfuric acid and water (30 mL) and heated at 90° C. for 12 h. The mixture was poured onto ice and the resulting yellow solid was collected by filtration and dried in vacuo to give (0.7 g, 80% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05721234 |
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| Source dataset | uspto-grants-1998_02 |
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| ORD ID | ord-7d9b6278e0c3488f98762565d183a9e4 |
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| Source note | uspto-grants-1998_02 |
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