Hydrochloric Acid → HCID 19696169, compound

Participants

Reaction Steps

N-(5-Acetylamino-6-bromo-4-nitro-indan-2-yl)-acetamide (1 g, 2.8 mmol) was stirred in 3N HCl (80 mL) at reflux for 3 h. The resulting solid was collected by filtration and dried in vacuo. Additional material was obtained by evaporation of the filtrate to give a combined yield of 93% of the yellow orange product (0.8 g).

Provenance & Evidence