Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 863518Generated: October 30, 2026

Acetic Acid → HCID 19696199, compound

https://huagongshe.com/reaction/863518

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHCID 19696247HCID 19696247—
SolventHydrochloric AcidHCID 313—
ProductHCID 19696199HCID 19696199—

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 5-acetamido-6-bromo-2-carboxyethyl-4-nitroindane (7.1 g, 19 mmol) in acetic acid (25 mL) and 3N HCl (100 mL) was heated at 100° C. for 18 h. The mixture was concentrated by rotoevaporation, and the resulting orange solid was collected by filtration, washed with ether and dried to give the product (5.5 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05721234
Source datasetuspto-grants-1998_02
ORD IDord-25b840cacb644f12b1e059e1138fb8fa
Source noteuspto-grants-1998_02