Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 19696247 | HCID 19696247 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19696199 | HCID 19696199 | — |
Reaction Steps
A mixture of 5-acetamido-6-bromo-2-carboxyethyl-4-nitroindane (7.1 g, 19 mmol) in acetic acid (25 mL) and 3N HCl (100 mL) was heated at 100° C. for 18 h. The mixture was concentrated by rotoevaporation, and the resulting orange solid was collected by filtration, washed with ether and dried to give the product (5.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05721234 |
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| Source dataset | uspto-grants-1998_02 |
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| ORD ID | ord-25b840cacb644f12b1e059e1138fb8fa |
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| Source note | uspto-grants-1998_02 |
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