HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22882815, compound → HCID 67590336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22882815 | HCID 22882815 | — |
| Reactant | HCID 178478989 | HCID 178478989 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67590336 | HCID 67590336 | — |
Reaction Steps
In a manner analogous to that described in Example 11(iii), from 2.0 g (7.75 mmol) of 6,7,8,9-tetrahydro-N-methoxy-N-methylpyrido[1,2-a]indole-8(S)-carboxamide and 15 ml (30 mmol) of a 2M solution of cyclopentylmagnesium chloride in diethyl ether, there were obtained 1.1 g of cyclopentyl 6,7,8,9-tetrahydropyrido[1,2-a]indol-8(S)-yl ketone as a pale yellow solid of melting point 69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721230 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-a8fb18e1e27d424cb868ae85e1f7bf78 |
| Source note | uspto-grants-1998_02 |