HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54678585, compound → 7,8-Dihydropyrido[1,2-a]indol-9(6H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54678585 | HCID 54678585 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 7,8-Dihydropyrido[1,2-a]indol-9(6H)-one | HCID 15063393 | 99.8% |
Reaction Steps
A solution of 1.03 g of ethyl 6,7-dihydro-9-hydroxypyrido[1,2-a]indole-8-carboxylate in 20 ml of ethanol, 10 ml of water and 10 ml of concentrated hydrochloric acid was heated at 80° C. for 3 hours. The solvents were evaporated to give 740 mg of 7,8-dihydropyrido[1,2-a]indol-9(6H)-one of melting point 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05721245 |
| Source dataset | uspto-grants-1998_02 |
| ORD ID | ord-acefca05672f4d9689d62e9a41cede22 |
| Source note | uspto-grants-1998_02 |