反应详情

The procedure of Example 26 is repeated using 1.0 g of bis(chloromethyl)-4-methoxy-5-(phenylmethoxy)benzene and 0.6 mL of benzyl amine. This affords 0.74 g of the desired product as a beige solid. mp 94°-96° C. MS(FAB): m/z 346 (M+H). Calcd for C23H23NO2 0.05M CH2Cl2 : C=79.16, H=6.66, N=4.01 Found C=78.96, H=6.76, N=3.87