Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-n-Octyloxyphenylboronic Acid (contains varying amounts of Anhydride) → 2-Fluoro-3,6-bis (4-octyloxyphenyl)pyrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-n-Octyloxyphenylboronic Acid (contains varying amounts of Anhydride) | HCID 3977284 | — |
| 반응물 | 2-Bromo-3-fluoro-5-(4-octyloxyphenyl)pyrazine | HCID 21804633 | — |
| 생성물 | 2-Fluoro-3,6-bis (4-octyloxyphenyl)pyrazine | HCID 12130686 | 73.7% |
반응 단계
An analogous reaction to Example 1b of 2.00 g (5.25 mmol) of 2-bromo-3-fluoro-5-(4-octyloxyphenyl)pyrazine (prepared as described in Example 1a-1c) and 1.31 g (5.25 mmol) of 4-octyloxyphenylboronic acid gives 1.96 g of 2-fluoro-3,6-bis (4-octyloxyphenyl)pyrazine. ##STR18## The compound has the following phase sequence:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05562859 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-51e4d89e4c494358a4ba6cae0a56e442 |
| 출처 메모 | uspto-grants-1996_10 |