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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 864417Generated: October 30, 2026

2-Methylbenzaldehyde → HCID 54566374, compound

https://huagongshe.com/reaction/864417

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethylbenzaldehydeHCID 10722—
ReactantMethyl 2-azidoacetateHCID 4020482—
ProductHCID 54566374HCID 54566374—

Reaction Steps

Following the general procedure of PREPARATION 61 and making non-critical variations but starting with o-tolualdehyde (5.0 g), methyl azidoacetate (19.2 g), the title compound is obtained, NMR (300 MHz, CDCl3) 7.96, 7.26-7.18, 7.13, 3.92 and 2.36 δ.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05563142
Source datasetuspto-grants-1996_10
ORD IDord-587d8cd61640432aa20ee216a47548e2
Source noteuspto-grants-1996_10