HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluoroacetyl chloride → HCID 21477695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluoroacetyl chloride | HCID 9663 | — |
| Reactant | HCID 21477686 | HCID 21477686 | — |
| Product | HCID 21477695 | HCID 21477695 | — |
Reaction Steps
Following the general procedure of PREPARATION 101 and making non-critical variations but starting with fluoroacetyl chloride (0.94 g), 1-benzyloxycarbonyl-4-[3-amino-2-pyridinyl]piperazine (PREPARATION 100,3.0 g), the title compound is obtained, NMR (300 MHZ, CDCl3) 8.83, 8.65, 8.14, 7.38-7.32, 7.12, 5.17, 4.96, 3.70 and 3.07 δ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05563142 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-9c1b397700ca4151939bc2ddc6c2baf3 |
| Source note | uspto-grants-1996_10 |