Tert-Butylamine → HCID 21477643, compound

HRID 864428Notes

Reaction equation

HRID 864428 reaction equation
[C:1]([NH2:5])([CH3:4])([CH3:3])[CH3:2].[Cl:6][C:7]1[N:8]=[N:9][CH:10]=[C:11]([Cl:14])[C:12]=1Cl>>[Cl:6][C:7]1[N:8]=[N:9][CH:10]=[C:11]([Cl:14])[C:12]=1[NH:5][C:1]([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 6385Tert-ButylamineHCID 701113,4,5-Trichloropyridazine

Product 1

HCID 21477643HCID 21477643, compound

Procedure

Following the general procedure of PREPARATION 31 and making non-critical variations but starting with t-butylamine (66.5 ml), and 3,4,5-trichloropyridazine, the title compound is obtained, NMR (300 MHz, CDCl3) 8.50, 5.09, and 1.55δ.

Workup

  1. customthe general procedure of PREPARATION 31

Sources & evidence

ORD record
ord-8f0bd56af27849f59a363d7a50a7b2aa
Source dataset
uspto-grants-1996_10
Patent number
US05563142

Reaction notes

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