HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 489442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 19418857 | HCID 19418857 | — |
| Reactant | HCID 19418895 | HCID 19418895 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 489442 | HCID 489442 | — |
Reaction Steps
Following the general procedure of EXAMPLE 16 and making non-critical variations but starting with 6-methoxy-7-methylindole-2-carboxylic acid (0.23 g), 1-(3-ethyl-2-pyridinyl)piperazine (0.24 g), 1,1'-carbonyldiimidazole (0.19 g) and THF (3 ml), the title compound is obtained, mp 162°-163°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05563142 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-990f85339767410f8186017783431b21 |
| Source note | uspto-grants-1996_10 |